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Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3)
  • Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3) 1

Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3)

Waiwai Kemika:

ʻĀpana Molekala C23H25NO4
Molar Mass 379.45
ʻO ka mānoanoa 1.238
Lae hehee 161-187 ℃
Lae Boling 602.9±38.0 °C(Wānana ʻia)
Ka nana aku ʻO ka pauka keʻokeʻo keʻokeʻo
pKa 3.89±0.10(Wanamua)
Kūlana Waihona Hoʻopaʻa ʻia i loko o kahi maloʻo, lumi wela

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Papa Hazard HOOLAHA

Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3) ʻIkepili

Hoʻohana ʻO ka Fluorene methoxycarbonyl D-cyclohexylglycine he lāʻau lapaʻau maʻamau a me ke kinikini waena, ʻo ka fluorenyl chloride (FMOC-Cl) he chloroformate. Hoʻohana ʻia ia e hana i ka fluorene methoxycarbonyl (hui FMOC) i loko o ka fluorene methoxycarbonyl carbamate FMOC carbamate, he hui pale amino maʻamau.
Hoʻomākaukau Ua hōʻike ʻia ka synthesis o ka fluorene methoxycarbonyl D-cyclohexylglycine i ka palapala. Ke hoʻohana nei i ka cyclohexyl bromide e like me ka mea maka, ma ke alo o ka sodium alkoxide, e hana ia i ka hopena alkylation me diethyl malonate, a laila hydrolyzes, acidifies, a me nā decarboxylates e loaʻa ai ka cyclohexyl acetic acid; ʻo ka mea hope e brominated a me ka ammonolysis DL-Cyclohexylglycine; ʻO ka hopena, loaʻa ka hopena acylation i mua o ka fluorene methoxycarbonyl chloride e loaʻa ai ka fluorene methoxycarbonyl D-cyclohexylglycine [1]. ʻO ke ala hoʻohālikelike synthesis penei:
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